 The synthesis of nanostructured copper and zinc oxides with unique properties and potential applications in various fields is analyzed, emphasizing the importance of laser-based methods for synthesizing oxide nanostructures, wavefront shaping techniques for precise control over light waves, and laser-induced thermochemical processes for creating and improving the properties of ZNO and CUO-based nanomaterials. The analysis shows that pulse-periodic laser treatment coupled with precise laser beam control using free-form diffractive optics presents novel opportunities for applications in optoelectronics, sensor technology, electronics manufacturing, and other fields. This article was authored by Sergei P. Merzin and Nikolai L. Kozansky.