Lab. R&D Chemical Reactor

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Uploaded by on Jul 31, 2011

chemical Reactor
The chemical reaction in which high molecular mass are formed from monomers is known as POLYMERIZATION.
· Reactor vessel capacity 25 L.
· All contact parts with the product made off S.S 316.
· Polymerization synthesis lab scale reactor with distillation system for emulsion, Solution and slurry phases.
· Instrumentation for online control of parameters by Programmable Logic Control and Digital Control System connected with reactor computer.
Technical Specifications
Temperature Range +5 ºC above ambient to 300 ºC with temp. Accuracy ± 1º C.
Electrically heated 4 KW heating power, Reactor vessel heating through Jacket.
Glass level gauge fitted with jacket to show thermal oil level in the jacket.
Reactor cooling System with internal cooling coil automatic controlled with solenoid valve system.
Pressure Gauge 100 Bar to show vessel pressure, pressure range 60 Bar.
Pressure regulator and pressure limit switch.
½ Hp 220 V Ac, Vacuum Pump with vacuum gauge of range 0 to -30 inHg, vacuum adjustable valve.
S.S gas inlet tube fitted in bottom of vessel replaceable.
Distillation assembly, reflux condenser fitted with reactor top plate/flange.
Steam stripper /distillation column fitted with collector column for recycling of monomers and extraction of by products.
Separate Condenser for vacuum distillations to attach with vacuum pump, glycerin filed vacuum gauge.
Circulation pump with adjustable flow rate fitted with reactor.
½ Hp Gear motor for stirring with three different change abele stirring blades, stirring speed 10-300 RPM. Inverter speed control and speed display.
Sample and bottom drain valves.
S.S Filter Sieve assembly 100 or fine Mesh fitted with out let valves.
Vent valve for pressure release.
Valve Connection for gas cover on vessel top as needed.
Monomers, Ingredients, Co Monomer and Water dosing 5 Liter capacity tanks two in No. with manual and automatic dose adjustable precise feeding pumps.
Washing/Polymer storage tank 20 L.
Solid input port with cap.
Light arrangement for material inspection in the vessel.
Vessel top plate with sensor ports and shaft coupling to attach gear motor.
Glass window at side of reaction vessel.
Silicon / Teflon seal for pressure sealing of top plate/flange and vessel.
S.S 304 Jacket for heating and temp. controlling of reaction vessel.
Ceramic wool insulation of exterior of vessel covered with S.S. 304.
Pressure release and pressure safety valve. Over pressure and temp. control for safety.
Cabinet for instrumentation and heavy sport S.S ring for working height level.

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