If I make nitrocellulose where you have to put cotton in sulfuric acid and then nitric acid.Can I dissolve the gun cotton in acetone, and get nitrocellulose Lacquer?
I'm confused. Is this TRUE nitrocellulose where you have to put cotton in sulfuric acid and then nitric acid? or is it just cellulose that has been dunked into a kno3 solution?
@japanesepoptart It is true nitrocellulose made by submersion in a solution of sulfuric acid and potassium nitrate, which converts to nitric acid in solution. I explain the process on grassrootsdiy(dot)com
@japanesepoptart Yes, more or less. It needs to be heated and condensed out of the solution to be purified, but can be used as is in solution to produce NC. Check my website.
@japanesepoptart You can also make nitrocellulose from a mixture of 45ml H2SO4 98% with 35ml HNO3 70%. I prefer using straight acids as the result is purer and you don't have to deal with dissolving the XNO3 (any nitrate salt will do-KNO3, NH4NO3, NANO3, etc.)
It's an azeotrope of water... so regular distilling won't purify it. The max. conc. through regular distilling is (actually) only 68%. Adding Sulfuric Acid or Magnesium Nitrate can bring it to 98% because those two compounds are dehydrating.
well i must say that ive NEVER heard about nitric acid above 70% but ive heard about oleum which is extremely concentrated sulfuric acid (165%?) a teacher from my class even worked with oleum like you use table salt in everyday life xD lucky guy.. and nikel metal (selfignites when its dry) and chloroform ^^ and mercury :D could be really cool to have such a job where you get in contact (no not directly in TOUCH with the stuff) with such advanced stuff.. (:
ok so here's a new question. first of all, ive made pretty good Nitrocellulose this way and even been able to use it to shoot a .38 cal bullet (very slow and unreliable) but i was wondering if you have made NC laquer with it? i have only used ping pong balls and smokeless powder. let me know.
@Jwdrummer5 for clarifycation, can u get nirtocellulose from pingpong balls and acetone? if dried and stuff correctly? i use the sulfuric acid and nitric acid method. I dont know too much about using pingpong balls.
hey i heard you could make it with kno3 and sulfuric acid but i never got it to work. same with the nitric acid sulfuric acid mix mabey i don't have the right temp. can anyone help?
i made a batch last night look at my vid i uploaded it was a lil slow cuz i didnt get the celloulose to soak it up is there a way i can lower the fumes the stuff is bad
kk cool what hard ware store would it be i called one next to my house and it was a ace and they dont have one so im gonna have to drive like an hour to get to the big city what store should i look for and what brand?
You'd probably need a higher concentration, or thoroughly evaporate the water.
The reason you need sulfuric acid is because it realy loves water. So much that it'll actualy get nitric acid to react and fall apart in a nitronium ion and water. The sulfuric acid takes the water and the nitronium ion reacts with the coton to form gun coton.
Now if there's too much water you can't realy get the sulfuric acid to "steal" the water from the nitric acid, so the reaction won't realy go.
is there a use for this as far as fireworks go.? its verry interesting dont get me wrong but because of who you are i never seen you use it in any of your vids yet.
It is useful as a star binder and a waterproof coating for fuse. The non pyrotechnic uses include smokeless gunpowder and many plastics. Pingpong balls, guitar pics, nail polish- The list goes on.
Sulfuric can be found in some heavy duty drain cleaner. Nitric can then be made from sulfuric and ammonium or potassium nitrate. That step is unnecessary though for the synthesis of nitrocellulose. Simply stir in a few cotton balls with 30ml of sulfuric and 20-25g of kno3 or nh4no3 and wait an hour or so. Then wash out the cotton balls with baking soda water or ammonia to clear out the acid. Careful of the vapors the acid gives off, do not breathe them in and do this process entirely outside.
why are you guys all distilling the nitric acid? i make nitroglycerin and nitrocellulose with AN(without distillation) and i think it would work with KNO3
Nope, the best way I've found is you take 30ml of 95%+ concentration sulfuric, stir in 20g of kno3 and add 2g of cotton balls. Stir every 20 minutes for an hour and then stir in another 5g of kno3 and let it sit for another half hour. Then rinse out what is now NC with water many times and then soak it in water with baking soda in it and add more baking soda till it stops fizzing, then rinse with water again and dry. it'll burn allot faster than the stuff in this video.
wat u just explained is that to just make 1 nc ball? or do u just add more cotton balls into that mixture? or do add more mixture depending on how much u want to make?....please further explain.
Just sulfuric and kno3, it's actually some of my slower stuff, I've had some pretty good results letting the solution sit for a couple hours with stirring every once in a while.
put strontium nitrate in it for me please?!
mcwario13 4 months ago
nice
sprengmeisterN 1 year ago
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If I make nitrocellulose where you have to put cotton in sulfuric acid and then nitric acid.Can I dissolve the gun cotton in acetone, and get nitrocellulose Lacquer?
vanessatroll 1 year ago
make that with 3,5kg... xD
187H4X0R187 1 year ago 4
I'm confused. Is this TRUE nitrocellulose where you have to put cotton in sulfuric acid and then nitric acid? or is it just cellulose that has been dunked into a kno3 solution?
japanesepoptart 1 year ago
@japanesepoptart It is true nitrocellulose made by submersion in a solution of sulfuric acid and potassium nitrate, which converts to nitric acid in solution. I explain the process on grassrootsdiy(dot)com
Nighthawkinlight 1 year ago
@Nighthawkinlight
WOEWOEWOEWOEWOE!!! STOP!
KNO3 + H2SO4 = NITRIC ACID?!?!?
If so, I wish I would have known that a LONG time ago >:(
japanesepoptart 1 year ago
@japanesepoptart Yes, more or less. It needs to be heated and condensed out of the solution to be purified, but can be used as is in solution to produce NC. Check my website.
Nighthawkinlight 1 year ago
@japanesepoptart
How do you make this again a ph of 7 ?
bas12345654321 9 months ago
@bas12345654321
You mean nitric acid? you neutralize it with a base solution like sodium hydroxide.
japanesepoptart 9 months ago
@japanesepoptart
Blind leading the blind.
NaOH destroys nitrocellulose. Sodium bicarb is what to use.
donnelrj01 8 months ago
@japanesepoptart You can also make nitrocellulose from a mixture of 45ml H2SO4 98% with 35ml HNO3 70%. I prefer using straight acids as the result is purer and you don't have to deal with dissolving the XNO3 (any nitrate salt will do-KNO3, NH4NO3, NANO3, etc.)
prometheustwin1970 1 year ago
@prometheustwin1970
Well, I prefer using pure chemicals too, but pigs will fly the day I get nitric acid :(
japanesepoptart 11 months ago
@japanesepoptart I guess you 're having a hard time getting conc. HNO3? If So, try artchemicalsdotcom. Or do you not Want to get Nitric acid?
prometheustwin1970 10 months ago
98,3% sufuric acid and 60-80% nitric acid or just only 95% nitric acid.
tuipale 2 years ago
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nitric acid only does up to 70%
bustincapz 2 years ago
no. nitric acid can be concentrated by destilling it.
NO2 gas can dissolve in H2O to form a max of 70% HNO3, but this acid can be destilled to 99%
Peterditaa 2 years ago
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Nitric Acid is an Azeotrope of water... it can't surpass 70% conc.
Distilling nitric acid would still result in a 70-30 boil off.
acsempronio 2 years ago
it makes the azeotrope with the sulfiuric acid, doesnt it?
you can get up to 98%. its called either red fuming nitric acid (if it has nitrogen dioxide impurities) or white fuming (if it doesnt).
and technically its 68% [: thats the max concentration you can get through the ostwald process.
wattapassa 2 years ago
It's an azeotrope of water... so regular distilling won't purify it. The max. conc. through regular distilling is (actually) only 68%. Adding Sulfuric Acid or Magnesium Nitrate can bring it to 98% because those two compounds are dehydrating.
acsempronio 2 years ago
dont you mean magnesium sulphate?
but yeah, your right. any dehydrating agent should work, as long as its not alkali, and it needs to be anhydrous.
wattapassa 2 years ago
seems H2O2 can convert NO2 to HNO3
2NO2 + H2O2 ----> 2HNO3
adriiPortillo 2 years ago
...and distilling from a dry alkali metal nitrate + dehidratating agent yields 99% nitric :)
adriiPortillo 2 years ago 3
Thats the azeotrope which means you cant get higher concentrations by just destilating.
Hismathefirst 2 years ago
well i must say that ive NEVER heard about nitric acid above 70% but ive heard about oleum which is extremely concentrated sulfuric acid (165%?) a teacher from my class even worked with oleum like you use table salt in everyday life xD lucky guy.. and nikel metal (selfignites when its dry) and chloroform ^^ and mercury :D could be really cool to have such a job where you get in contact (no not directly in TOUCH with the stuff) with such advanced stuff.. (:
antiswattt2 2 years ago
ok i read on wiki that it DOES go over 70% just not sold that many places i guess.. :S
antiswattt2 2 years ago
lemme see and stop hatin you bitches
bustincapz 2 years ago
lol ^^ in NurdRage's video he made fuming nitric acid.. = really concentrated
antiswattt2 2 years ago
yea i saw that you a fan too :P
bustincapz 2 years ago
ofc..
antiswattt2 2 years ago
@antiswattt2 NurdRage has some really good videos =P
oXFalconXo 1 year ago
LOL
NUNNAP 2 years ago
ok so here's a new question. first of all, ive made pretty good Nitrocellulose this way and even been able to use it to shoot a .38 cal bullet (very slow and unreliable) but i was wondering if you have made NC laquer with it? i have only used ping pong balls and smokeless powder. let me know.
Jwdrummer5 2 years ago
Yeah it works fine.
Nighthawkinlight 2 years ago
@Jwdrummer5 It should work but I believe you must add camphor oil to it to plasticize it.
japanesepoptart 1 year ago
@Jwdrummer5 for clarifycation, can u get nirtocellulose from pingpong balls and acetone? if dried and stuff correctly? i use the sulfuric acid and nitric acid method. I dont know too much about using pingpong balls.
ghk913 10 months ago
hey i heard you could make it with kno3 and sulfuric acid but i never got it to work. same with the nitric acid sulfuric acid mix mabey i don't have the right temp. can anyone help?
3981784 2 years ago
Read previous comments.
Nighthawkinlight 2 years ago
sorry i know what it's like when people comment the same question like 100 times
3981784 2 years ago
No problem
Nighthawkinlight 2 years ago
i made a batch last night look at my vid i uploaded it was a lil slow cuz i didnt get the celloulose to soak it up is there a way i can lower the fumes the stuff is bad
flashsn1pe 2 years ago
The fumes are part of the deal. Just work upwind.
Nighthawkinlight 2 years ago
Ore use a respirator.....
zink905 2 years ago
How do you make gun cotton? EMail me if you don't want to talk about it in public
magnum9987 2 years ago
where do i get the sulfuric acid drain opener? and is this basicly flash cotton? im thinking of using it as magic trick effects
flashsn1pe 2 years ago
Many hardware stores carry sulfuric drain opener. Yes this is flash cotton.
Nighthawkinlight 2 years ago
kk cool what hard ware store would it be i called one next to my house and it was a ace and they dont have one so im gonna have to drive like an hour to get to the big city what store should i look for and what brand?
flashsn1pe 2 years ago
True Value usually has a good selection. The brand I found with highest conc. is Rooto.
Nighthawkinlight 2 years ago
I guess when I use less pure (30%?) sulfuric acid.. Only the ratios change because the other 70% is just H2O?
The water will just evaporate during the process? Thanx
o0Dreamlike0o 2 years ago
I'm not sure if that conc. will work, but you can try.
Nighthawkinlight 2 years ago
You'd probably need a higher concentration, or thoroughly evaporate the water.
The reason you need sulfuric acid is because it realy loves water. So much that it'll actualy get nitric acid to react and fall apart in a nitronium ion and water. The sulfuric acid takes the water and the nitronium ion reacts with the coton to form gun coton.
Now if there's too much water you can't realy get the sulfuric acid to "steal" the water from the nitric acid, so the reaction won't realy go.
Buionics 2 years ago
thnxs<-- explains everything!
propyropower 2 years ago
can this stuff detonate if confined?
1calman1 2 years ago
It is all in how it is initiated. It is the base for smokeless gunpowder, as well as a huge number of other applications, mostly in plastics.
Nighthawkinlight 2 years ago
can you pm me on you recipy? yours burn very fast even in a ball my stuff burns fast but not that fast in a ball.
tntskull 3 years ago
Read the rest of the comments on this video.
Nighthawkinlight 3 years ago
Could you please make tutorial on how to make NC
BombMaker0312 3 years ago
:o firery
leroy5500 3 years ago
Can nitro cellulose 25% from SL be used in anyway for this process.
poprocz 3 years ago
You mean piled up and lit on fire? No it can't.
Nighthawkinlight 3 years ago
is there a use for this as far as fireworks go.? its verry interesting dont get me wrong but because of who you are i never seen you use it in any of your vids yet.
oahuguy 3 years ago
It is useful as a star binder and a waterproof coating for fuse. The non pyrotechnic uses include smokeless gunpowder and many plastics. Pingpong balls, guitar pics, nail polish- The list goes on.
Nighthawkinlight 3 years ago
try lifting a shell with nitrocellulose or nitrocellulose powder,start with 1 inch shells to get it right though
pyrogeniuses 3 years ago
To pricey for that.
Nighthawkinlight 3 years ago
oh,dang then lol
pyrogeniuses 3 years ago
If my drain cleaner contains sulfuric acid,other acid and some other stuff will it work?
van5003 3 years ago
It's dangerous to use unknown chemicals. Find the purest acid you can buy. I use rooto brand drain cleaner.
Nighthawkinlight 3 years ago
Thank you.
van5003 3 years ago
So I need to evaporate the water that is i the acid to make it concentrated.
van5003 3 years ago
Or just buy a bottle of concentrated sulfuric in the form of drain cleaner for ~$8 a bottle...
Nighthawkinlight 3 years ago
do you think that sulfuric acid from my acid battery will work ?
van5003 3 years ago
Perhaps, though it will take longer than usual.
Nighthawkinlight 3 years ago
No it wont work. The acid serves to dehydrate the mixture so 80% + concentration must be used. Just boil your acid down to the required volume.
donnelrj01 3 years ago
dose any one know were to find cellulose
booga4life 3 years ago
Cotton is almost pure cellulose.
Nighthawkinlight 3 years ago
also do u know were to find Nitric acid and sulfuric acid in house hold objects
booga4life 3 years ago
Sulfuric can be found in some heavy duty drain cleaner. Nitric can then be made from sulfuric and ammonium or potassium nitrate. That step is unnecessary though for the synthesis of nitrocellulose. Simply stir in a few cotton balls with 30ml of sulfuric and 20-25g of kno3 or nh4no3 and wait an hour or so. Then wash out the cotton balls with baking soda water or ammonia to clear out the acid. Careful of the vapors the acid gives off, do not breathe them in and do this process entirely outside.
Nighthawkinlight 3 years ago
thanks this really helped me
booga4life 3 years ago
will Hcl work instead of sulfuric acid?
NH4NO3CH3NO2 3 years ago
Not likely. Just buy a bottle of sulfuric, about $8 for a liter.
Nighthawkinlight 3 years ago
What retail did you get your H2SO4?
Home Depot
I would suspect you need some papers to get ~90% sulfiric.
ventsi 3 years ago
98% sulfuric, $9 a liter last I checked. In the form of professional drain cleaner. Found it at a true value hardware store, Rooto brand.
Nighthawkinlight 3 years ago
Thanks im going to be on my way to HomeDepot to check.
ventsi 3 years ago
Home Depot doesn't sell sulfuric acid based drain openers.
Cyf531 2 years ago
True but OSH and Lowes do,]
I got mine at OSH
ventsi 2 years ago
where do you get sulfuric acid
theartilerysheller1 3 years ago
Put it under pressure and youll see : BOOM !
idricool 4 years ago
Well there are better ways, but yeah..
Nighthawkinlight 4 years ago
yeah if it works there's no reason to stop.
Nighthawkinlight 4 years ago
hmm, pretty cool, i've never gotten the vapors to flow through a hose by their own at a normal temperature
Nighthawkinlight 4 years ago
hmm, interesting, that is what it would be. how did you collect them? also, if it is nitric, you should have put it on more cotton for some more NC
Nighthawkinlight 4 years ago
why are you guys all distilling the nitric acid? i make nitroglycerin and nitrocellulose with AN(without distillation) and i think it would work with KNO3
silendshade 4 years ago
Because nitric makes a much better product, you can tell the difference with purified NC.
Nighthawkinlight 4 years ago
no problem, I've found most sulfuric drain openers work well
Nighthawkinlight 4 years ago
KNO3 really ain't that bad for NC. Pretty nice. Although straight acids are easier and faster to work with.
Uberownager 4 years ago
Nope, the best way I've found is you take 30ml of 95%+ concentration sulfuric, stir in 20g of kno3 and add 2g of cotton balls. Stir every 20 minutes for an hour and then stir in another 5g of kno3 and let it sit for another half hour. Then rinse out what is now NC with water many times and then soak it in water with baking soda in it and add more baking soda till it stops fizzing, then rinse with water again and dry. it'll burn allot faster than the stuff in this video.
Nighthawkinlight 4 years ago
wat u just explained is that to just make 1 nc ball? or do u just add more cotton balls into that mixture? or do add more mixture depending on how much u want to make?....please further explain.
piroflash93 4 years ago
2g worth of cotton added to 25g kno3 and 30g sulfuric. that's enough for what is in the video.
Nighthawkinlight 4 years ago
Just sulfuric and kno3, it's actually some of my slower stuff, I've had some pretty good results letting the solution sit for a couple hours with stirring every once in a while.
Nighthawkinlight 4 years ago
Did you use nitric acid or AN?
slither888 4 years ago