Thank you for your comments regarding the OH / CH2 peaks. The chemical shift of OH is very dependent on solvent and other experimental conditions so cannot be assigned by chemical shift alone.
Very awesome video, I just had a lecture on these exact subjects and this shed some serious light on what it all looks like in the laboratory setting. It kind of sucks to learn about how to read the charts and what everything means without even having a clue what the NMR machine looks like. Thank you!
@kingfinnc yup, youre right...I was watching some other videos on this same subject and they showed that the OH chemical shift was in the 4-5 ppm range...idk what is up with this one in this vid...lol
I noted that in this video, the OH shift appears at around 1.6 ppm... However, shouldn't the OH proton be more downfield since it experiences more deshielding due to oxygen? The splitting is accurate because OH hydrogens are usually singlets... The CH2 protons do not experience as much of an inductive effect as the H bonded with the oxygen.
The H chemical shift of OH should appear near 5.3 ppm
That's a bruker biospin/bioshield 300 Mhz, the higher the frequency the higher the magnetic field and trivially speaking the machine gets bigger. At the 800 respec. 1100 Mhz unit at our institute you really need stairs to get the sample in to the probe. To measure other nuclei you just need a "special" probehead (not really explained in this video) but basically you're right, any "magnetic" nuclei can be measured with any NMR machine
Thank your for upload! Do you know abought Nuclear spin tomografy? Also did you knew that you do not need nitrogen jacket if you have some special thermo foil wound around the helium jacket?
Wow this is really amazing. This video clarified a lot, thanks. Any idea how "old" this NMR machine is? From what I know, previously these machines required stairs to reach the top of the machine. Or is this version much smaller as this machine only does proton NMR?
I think this one can detect other isotopes, but the massive ones work with smaller samples, so for like forensics you might use a big one because you only have a small sample, and therefore need a bigger magnet. i think this is why.
Good video, but not exactly what I was looking for. I was looking more for a video that focused more on interpreting graphs and being able to draw molecules from that. But I very much enjoyed the background to how the experiment is done, thanks.
This kind of video is so practical!! Thank you for uploading.
azzuri98 1 month ago
A great video.
shbsul 2 months ago
shoudnt he be wearing gloves when handling the hydomethene
junior1984able 9 months ago
Spin Spin Splittting is my new favourite scientific term :)
jewboyjewboy1 10 months ago
very good video.
juschet8 1 year ago
These clips are superb.
ubiquim 1 year ago
Thank you for your comments regarding the OH / CH2 peaks. The chemical shift of OH is very dependent on solvent and other experimental conditions so cannot be assigned by chemical shift alone.
wwwRSCorg 1 year ago
I think they have shown the peak for CH2 at 2.5 instead of showin at 1.6 and opposite for OH.
Atleast the videos from RSC should be atleast reviewed onced before posting!
reaperwalter15 1 year ago
Good video..
deeekaaa21 1 year ago
Very awesome video, I just had a lecture on these exact subjects and this shed some serious light on what it all looks like in the laboratory setting. It kind of sucks to learn about how to read the charts and what everything means without even having a clue what the NMR machine looks like. Thank you!
alexnkassiesavage 1 year ago
I did this work for my exam of chemical analist on MLO. I want to know where can I do the studie to become NMR specialist? plz replie
1986liberty21 1 year ago
i hope my school can afford to purchase 1 unit of nmr. its very effective for structural elucidation...
glianx 1 year ago
i don't know if i'm wrong, but i think i'm not:
but the chemical shift of the shown H in the OH-group has to be higher than the ones of the CH2-Group ?!? must be at 5,5ppm or somewhere near that.
Greez from germany
kingfinnc 1 year ago
@kingfinnc yup, youre right...I was watching some other videos on this same subject and they showed that the OH chemical shift was in the 4-5 ppm range...idk what is up with this one in this vid...lol
free0fight 1 year ago
@kingfinnc no -ch2 gp is linked to electronegative atom so the value is higher than OH
pratik968 1 year ago
H1 NMR of ethanol:
I noted that in this video, the OH shift appears at around 1.6 ppm... However, shouldn't the OH proton be more downfield since it experiences more deshielding due to oxygen? The splitting is accurate because OH hydrogens are usually singlets... The CH2 protons do not experience as much of an inductive effect as the H bonded with the oxygen.
The H chemical shift of OH should appear near 5.3 ppm
newaaliyah 1 year ago
That's a bruker biospin/bioshield 300 Mhz, the higher the frequency the higher the magnetic field and trivially speaking the machine gets bigger. At the 800 respec. 1100 Mhz unit at our institute you really need stairs to get the sample in to the probe. To measure other nuclei you just need a "special" probehead (not really explained in this video) but basically you're right, any "magnetic" nuclei can be measured with any NMR machine
kxosz9 2 years ago
Thank your for upload! Do you know abought Nuclear spin tomografy? Also did you knew that you do not need nitrogen jacket if you have some special thermo foil wound around the helium jacket?
Subspace4d 2 years ago
Wow this is really amazing. This video clarified a lot, thanks. Any idea how "old" this NMR machine is? From what I know, previously these machines required stairs to reach the top of the machine. Or is this version much smaller as this machine only does proton NMR?
Cheers
JanAap04 2 years ago
I think this one can detect other isotopes, but the massive ones work with smaller samples, so for like forensics you might use a big one because you only have a small sample, and therefore need a bigger magnet. i think this is why.
mptmatthew 2 years ago
its really helpful...
thanks a lot:)
nehajohar 2 years ago
very nice
thanks
Kilozro 2 years ago
what about slicon-29?
maglight117 2 years ago
Good video, but not exactly what I was looking for. I was looking more for a video that focused more on interpreting graphs and being able to draw molecules from that. But I very much enjoyed the background to how the experiment is done, thanks.
MarcusDiMarco7 2 years ago 12
I love Bruker :-).
AtomicCactus 2 years ago
wow, it's really useful stuff.
Thanks so much for it !
DreamerJH87 2 years ago
This is brilliant!!! It was so well explained!!
But I'm still a bit confused about the peak splitting and n+1 rule!! Can someone explain please? (Textbooks make it more complicated)
irizarxyz 2 years ago
trichloroMEE-thane
Lol. I've never heard it pronounced that way and I've had a TA how pronounced carbocation like carbo-cation.
noinlair 2 years ago
lol ive got a mid sem on this innnn 10 hours time
07TonzPau 2 years ago
WOw, I really wish I found this video sooner! Thank you so much!
flyinghakusai 2 years ago
very helpful!
yh458 2 years ago
Thanks so much
plenarak 2 years ago
This is great. I can't lack the word to express my thx 5/5
yes4me 3 years ago 2
this is so cool, finally put my lecture into an experiment
fh1mahfanzai 3 years ago 2
well done
Leviathan42 3 years ago 8
nice
farhmoha 3 years ago
Thanks so much for posting :)
macmenmen 3 years ago
Thanks for sharing, this is perhaps the best video I've seen about basics of NMR; it is very well and concise explained.
myusername20202020 3 years ago