I have more. I was considering trying to save it, but it wasn't worth setting up the distillation apparatus for that much. Also, I'd have to repurify and dry the recovered chloroform before adding it back to the stock.
I might try recrystallizing it in a nonpolar solvent like chloroform by dissolving it into the chloroform, filtering out any insoluble components, and then boiling off the chloroform or allowing it to evaporate on its own. There would probably be significant mechanical loss, though, and this would, in all likelihood, only be worth it with a larger quantity of caffeine.
Using that huge amount of tea meant that I couldn't reasonably get all the liquid tea off the tea leaves. Most of it was still absorbed into the leaves after I decanted the water off. If I had used less, I could have been more careful about extracting all the caffeine off the leaves, and then getting all the liquid tea pressed off the leaves. It was only large relative to my scale of glassware; if I had bigger glassware, I could have done more with the same percent yield.
But if it's toxic, and you can't use it, then why did you make it? It seems kinda pointless.
rocketpro22 2 months ago
Now snort it...
meeatfood2 2 months ago
Pure caffine is white, u must have done the exp wrong
askar4kill 2 months ago
now do nicotine...nah just kidding : )
MisterNickOtine 3 months ago
Where are you, like on a boat or something?
Aazerel 8 months ago
Ethyl acetate? That is a reasonable substitute for what you are using know.
MrTechGuy1995 1 year ago
why take the caffeine out if you have no intent to consume it???
Dudethatstrippin 1 year ago
You could sublime it, NurdRage style!
yellowmetalcyborg 1 year ago
Try doing the same thing with Tobacco....see if you can get an extract.
hawk1buster 1 year ago
A nice procedure!
Will you try to purify the caffeine? Perhaps sublime it?
DoktorKlawonn 1 year ago
@DoktorKlawonn
We have no plan to, because we have no real use for the caffeine anyway.
ReactionFactory 1 year ago
@ReactionFactory
Oh, it's a pitty then you didn't recover the chloroform
DoktorKlawonn 1 year ago
@DoktorKlawonn
I have more. I was considering trying to save it, but it wasn't worth setting up the distillation apparatus for that much. Also, I'd have to repurify and dry the recovered chloroform before adding it back to the stock.
ReactionFactory 1 year ago
@ReactionFactory
better extract cocaine from coca leaf then
jammmon 6 months ago
and I didnt see any caffeine. You should purify it man.
Put that powder into a glass with a 100 ml water and 10 gr of sodium carbonate. Shake.
The caffeine base should precipitate out of the water, filter or freeze.
Dry it, and wash it with more water, it won't dissolve.
Then smoke it and blow your heart up
jammmon 6 months ago
do you also have suggestions on further extracion for a more pure sample?
tjiddles25 1 year ago
@tjiddles25
I might try recrystallizing it in a nonpolar solvent like chloroform by dissolving it into the chloroform, filtering out any insoluble components, and then boiling off the chloroform or allowing it to evaporate on its own. There would probably be significant mechanical loss, though, and this would, in all likelihood, only be worth it with a larger quantity of caffeine.
ReactionFactory 1 year ago
You said,
One could either use a tiny amount of tea, and get a pretty reasonable yeild,or a large amount of tea to get a bad yeild.....
May you explain?
kuro96inlaila 1 year ago
@kuro96inlaila
Using that huge amount of tea meant that I couldn't reasonably get all the liquid tea off the tea leaves. Most of it was still absorbed into the leaves after I decanted the water off. If I had used less, I could have been more careful about extracting all the caffeine off the leaves, and then getting all the liquid tea pressed off the leaves. It was only large relative to my scale of glassware; if I had bigger glassware, I could have done more with the same percent yield.
ReactionFactory 1 year ago
Nice view off the deck!
ytmachx 1 year ago
Nothing better than a line of caffeine in the morning!
tk0145 1 year ago
Glad to see it went well, yay, another caffeine video!
hkparker 1 year ago
I'd love to extract the caffeine out of Jolt cola for those mornings when I need a boost. Good. Thanks for sharing.
jeriellsworth 1 year ago
@jeriellsworth At that rate, you may as well just buy caffeine pills.
TickyTack23 1 year ago
@TickyTack23 Yes, but that takes all of the science fun out of it.
jeriellsworth 1 year ago
great video
coolliger 1 year ago
No sound? :(
Serostern 1 year ago
Nice video!
yellowmetalcyborg 1 year ago